Lab Single Layer Glass Reactor
Detail
This equipment is composed of electric constant speed stirring system, condensation, dropping system and heating bath. While stirring the materials, the bath heats the materials in the kettle. The evaporation efficiency can be increased under vacuum conditions ( a vacuum device need to be connected). The solvent vapor is cooled into liquid when passing through the glass condensing coil (a cooling device need to be connected), which can be refluxed into the kettle. It can also be recycled in collection flask.
Basic Configuration
• The parts in contact with the material are all made of high borosilicate glass (expansion coefficient 3.3) and PTFE materials, which have stable performance and are not easy to react with the materials.
• The main stent is made of cold plate anti-corrosive spray + aluminum alloy. And the bath is made of stainless steel.
• ON-OFF tilt switch to control stirring and heating.
• Electronic stepless speed regulation, fine-adjustment through knobs, speed box digital displaying speed.
• Constant temperature bath with temperature digital display, K-type sensor at bottom of bath + stainless steel probe.
• The stirring system uses ceramic bearings and mechanical seal to prevent the stirring rod from wearing out.
• Vacuum pressure gauge shows real-time vacuum indicated by pointer.
• Crescent-type stirring paddle, 304 stainless steel + PTFE stirring blade. The material of the stirring rod is 304 stainless steel, and it is wrapped in PTFE tube outside.
• Stirring, heating two fuses safety protection.
Products Parameter
| Model | F-100L | |
| Reactor volume | 100L spherical shape | |
| Voltage/Frequency | Stirring 220V 50Hz/110V 60Hz; Heating bath 380V/50HZ | |
| Stirring motor power | 200W1/3 | |
| Heating power | 12KW | |
| Stirring speed | 0-450rpm/min | |
| Temperature range of reactor | -80ºC~ +250ºC | |
| Temperature measuring accuracy | ±1ºC | |
| Vacuum | 0.098Mpa | |
|
Kettle body |
Stirring port | Φ205mm kettle lid with flange port Φ80 flange stirring port |
| Condensation reflux port | 50# ball mill port | |
| Port of constant pressure funnel | 34# standard port | |
| Pressure relief port | 34# standard port | |
| Temperature measuring port | Φ45 flange port | |
| Solid material feeding port | Φ125mm flange port supporting PTFE cap | |
| Bottom discharging port | Φ80mm flange port | |
| Stirring paddle | Φ17×1000H(mm) blade 190mm | |
| Condenser dimension | Φ120*600H(mm) lower Φ60 flange port | |
| Condensation area | 0.5m2 | |
| Dean-stark | Upper Φ60 flange port; left 50# ball mill stopper | |
| Volume of constant pressure funnel | 2L, upper 29# Standard port with glass stopper; lower 34#standard stopper | |
| Pressure relief valve | 34# standard plug valve; air outlet(pagoda joint)with 12mm outer diameter | |
| Material discharging valve | Φ80 flange port; Φ33mm material discharge hole; oblique discharge port(pagoda joint)Φ34mm; 350mm from the ground | |
| Vacuum nozzle | Pagoda joint with 12mm outer diameter | |
| In and out circulating nozzle of condenser coil | Pagoda joint with 15mm outer diameter | |
| Bath dimension | Φ700×400H(mm) | |
| Overall dimension(W*D*H) | 880×800×1850mm | |
| Net weight | 108KG | |
| Packing dimension | 1870×850×1010mm wooden package 1.61m³ | |
| Packing weight | 159KG | |
