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50L Explosion Proof Single Layer Glass Reactor

Short Description:

This equipment is composed of electric constant speed stirring system, condensation, dropping system and heating bath. While stirring the materials, the bath heats the materials in the kettle. The evaporation efficiency can be increased under vacuum conditions ( a vacuum device need to be connected). The solvent vapor is cooled into liquid when passing through the glass condensing coil (a cooling device need to be connected), which can be refluxed into the kettle. It can also be recycled through the lower valve of the dean-stark. When the reaction is completed, the material can be discharged from the side outlet at the bottom of the kettle.

This series of products need to be equipped with a vacuum device, a cooling circulating device, etc. to form a system devices.


  • Model: EXF-50L
  • Reactor volume: 50L spherical shape
  • Voltage/Frequency: Stirring 220V50HZ/110V 60Hz; Heating bath 380V/50HZ
  • Stirring speed: 0-1400rpm/min
  • Reactor temperature range: -80℃~ +250℃
  • Product Detail

    Product Tags

    Main Features

    • The parts in contact with the material are all made of high borosilicate glass (expansion coefficient 3.3) and PTFE materials, which have stable performance and are not easy to react with the materials.

    • The main stent is made of cold plate anti-corrosive spray + aluminum alloy. And the bath is made of stainless steel.
    • Glass + PTFE material discharging valve, side material discharge without effusion.
    • Frequency converter speed regulation, explosion-proof switch, fine adjustment through knob, explosion-proof box with dual display function, which can digital display speed and material temperature in kettle.

    • Constant temperature bath with temperature digital display, K-type sensor + stainless steel probe at bottom of bath.• The stirring system uses ceramic bearings and mechanical seal to prevent the stirring rod from wearing out.

    • Using PT100 temperature sensor, 304 stainless steel material, wrapped in transparent PTFE tube, double anti-corrosion.

    • Vacuum pressure gauge shows real-time vacuum by pointer.

    • Crescent-type stirring paddle, 304 stainless steel + PTFE stirring blade. The material of the stirring rod is 304 stainless steel, and it is wrapped in PTFE tube outside.

    • There is a water discharge valve at the bottom of the bath to facilitate liquid discharge

    • There is a universal wheel with brake at the bottom of the equipment, which can be moved as a whole and be operated conveniently.

    • Stirring, heating two fuses safety protection

     Explosion-proof motor, explosion-proof aluminum shell of frequency converter, explosion-proof aluminum shell of bath controller, explosion-proof tube with cable.

    Parameters

    Model EXF-50L
    Reactor volume 50L spherical shape
    Voltage/Frequency Stirring 220V50HZ/110V 60Hz; Heating bath 380V/50HZ
    Stirring motor power EX180W
    Heating power 8KW
    Stirring speed 0-1400rpm/min
    Reactor temperature range -80℃~ +250℃
    Temperature measuring accuracy ±1℃
    Vacuum 0.098Mpa
     

     

    Kettle body

    Φ470mm

    7 ports

    Stirring port Φ80mm flange port
    Condensation reflux port 50# ball mill port
    Port of constant pressure funnel 34# standard port
    Pressure relief port 34# standard port
    Temperature measuring port Φ45 flange port
    Solid material feeding port Φ125mm flange port supporting PTFE cap
    Bottom discharging port Φ80mm flange port
    Stirring paddle Φ17×900H(mm)  blade 190mm
    Condenser dimension Φ100*700H(mm)  lower Φ60 flange port
    Condensing area 0.4
    Dean-stark Upper Φ60 flange port; left 50# ball mill stopper
    Volume of constant pressure funnel 2L, upper 29# Standard port with glass stopper; lower 34#standard stopper
    Pressure relief valve 34# standard plug valve; air outletpagoda jointwith 12mm outer diameter
    Material discharging valve Φ80 flange port; Φ33mm material discharge hole; oblique discharge portpagoda jointΦ34mm;  350mm from the ground
    Vacuum nozzle Pagoda joint with 12mm outer diameter
    In and out circulating nozzle of condenser coil Pagoda joint with 15mm outer diameter
    Bath dimension Φ550×320H(mm)
    Overall dimension(W*D*H) 940×640×2130mm
    Net weight 65KG
    Packing dimension 1370×790×980mm wooden package 1.06m³
    Packing weight 112KG

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